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By J R Hanson; Royal Society of Chemistry

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Chim. Pays-Bas, 1979, 98, 5 2 . H. Sekizaki, M. Ito, and S. Inoue, Bull. Chem. , 1978, 51, 3663. H. Sekizaki, M. Ito, and S. Inoue, Bull. Chem. , 1978,51, 2439. H. Sekizaki, M. Ito, and S. Inoue, Chem. , 1978, 1191; Bull. Chem. , 1979, 52, 2161. c. Scheme 26 A number of model esters related to lac resin have been prepared. 87 In an approach to the synthesis of cedrene (152), the intramolecular photocycloaddition of the dienone (150) was carried out at low temperature. 88Further work is required to bring about the rearrangement of a derivative of (151) to give cedrene.

Sect. B, 1978, 16, 20, 23. 91 92 93 94 B. Tomita and Y. Hirose, Phytochemistry, 1973, 12, 1409. P. J. Carrol, E. L. Ghisalberti, and D. E. Ralph, Phytochemistry, 1976, 15,777. S. Manabe, K. Wakamatsu, Y. Hirata, and K. Yamada, Tetrahedron, 1979, 35, 1925. H. J. Liu and W. H. Chan, Can. J. , 1979, 57,708. ” For compounds belonging to the so-called isocedrane class, see p. 99. 95 K. Rajendran, S. K. Paknikar, G. K. Trivedi, andS. C. Bhattacharyya, IndianJ. ,Sect. B, 1978, 16,4. r. "' A (172) (173) R (174) R = = H OH M.

Pharm. , 1978, 26, 2543. R. F. Raffauf, M. P. Pastore, C. J. Kelley, P. W. Le Quesne, I. Miura, K. Nakanishi, J. Finer, and J. Clardy, J. Am. Chem. ,1978, 100, 7437. A. Matsuo, H. Nozaki, M. Nakayama, Y. Kushi, S. Hayashi, T. Komori, and N. Kamijo, J. Chem. ,Chem. , 1979, 174. M. Namikawa, T. Murae, and T. Takahashi, Bull. Chem. , 1978, 51, 3616. Sesqu iterpen a ids 39 (246) (247) (248) (252)-(256), whose mode of formation via the carbonium ion (25 1)is illustrated in Scheme 36. In recent years humulene has been viewed as a focal biogenetic precursor of an ever-increasing number of tricyclic sesquiterpenoids.

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